If the reaction doesn't go to completion, you will have aldehyde starting material present. how would you identify this impurity most easily by 1h nmr?

Question

Chemistry

Colt Byrd

1 January, 19:49

If the reaction doesn't go to completion, you will have aldehyde starting material present. how would you identify this impurity most easily by 1h nmr?

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Jordon David · Answer 1

- If the reaction does not go to completion, the presence of aldehyde can be identify easily by looking at the aldehydic proton peak in the range of 10 - 9 ppm (Chemical shift value).

- Aldehydic proton has a high value of chemical shift due to magnetic anisotropy so when looking at the most de-shielded proton we will found a signal or peak at 9-10 ppm corresponding to the proton of aldehyde